Crystal structure of 3'-formyl-benzo-15-crown-5, C15H20O6
نویسندگان
چکیده
منابع مشابه
Synthesis, Crystal Structure and Electrochemical Properties of a New Adduct of Benzo-15-crown-5 and H3PMo12O40
A new crown ether-POM (POM = polyoxometalate) adduct with the molecular formula [(C14H20O5)4(H3O)3]PMo12O40 · 0.5CH3CN (1) was isolated from the mixed solvent of acetonitrile and methanol. The adduct is constructed from Keggin [PMo12O40]3− anions and [(C14H20O5)(H3O)] and [(C14H20O5)2(H3O)] cations via electrostatic and hydrogen bonding interactions. The supramolecular interactions combine the ...
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The title compound, [Sr(C(14)H(20)O(5))(2)](I(3))(2), obtained by slow evaporation of an ethanol/dichloro-methane solution (1:1) of SrCl(2), benzo-15-crown-5 and I(2), is built of sandwich-like [Sr(benzo-15-crown-5)(2)](2+) cations and isolated linear I(3) (-) anions which are arranged in alternating layers parallel to (010). The triiodide anions are located in general positions, whereas the ca...
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In this work, we report a new hybrid nanomaterial based on the immobilization of 4-formyl benzo-9-crown-3 ether (FB9C3) onto the mesopores of MCM-41. First, the mesoporous molecular sieve MCM-41 was covalently grafted with 3-aminopropyl triethoxysilane to give aminopropyl modified MCM-41 (AmpMCM-41). Reaction of this material with FB9C3 afforded the B9C3-AmpMCM-41 hybrid nanomaterial. The prepa...
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Complexes of benzo-15-crown-5 macrocycle with Li+ and Cs+ ions were investigated by 7Li and 133Cs NMr in a number of nonoqueous solutions. The resulting 1:1 complex with Li+ ion was found to be much more stable than that with Cs+ ion. With the exception of pyridine solutions the stabilities of the complexes varied inversely w...
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The coextraction of water with benzo-15-crown-5 (B1SC5), benzo-18-crown-6 (B18C6) and the B18C6-K+ complex into seven low-polar solvents, i.e., carbon tetrachloride (CTC), chloroform (CF), dichloromethane (DCM), 1,2-dichloroethane (1,2-DCE), benzene (BZ), chlorobenzene (CB) and o-dichlorobenzene (o-DCB), has been investigated. The mean hydration number, nH2O, of these solutes in the water-satur...
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ژورنال
عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures
سال: 2006
ISSN: 2197-4578,1433-7266
DOI: 10.1524/ncrs.2006.0175